Chemical Profile: Europe butyl acetate
USES
Four butyl acetates exist, but only normal butyl acetate
(n-butyl acetate) and iso-butyl acetate are of commercial
importance. The major outlet for n-butyl acetate (butac) is
as a solvent for lacquers because it gives good flow and
brush resistance when used in film-coating resins such as
cellulose nitrate, cellulose acetate butyrate, ethyl
cellulose, polystyrene (PS) and methyl methacrylate (MMA)
resins.
It is also widely used as a solvent in the preparation of
artificial leathers, textiles and plastics, as an extractant
for oils and pharmaceuticals, and as an ingredient for
perfumes and synthetic flavours. Butac and butanol can be
used as a dehydrating agent because they form a ternary
azeotrope with water.
SUPPLY/DEMAND
European supply of butac was limited for much of 2017 due to
a force majeure declared by BASF in October 2016 following an
explosion and shutdown of its plant in Ludwigshafen, Germany.
In addition, OXEA had an unplanned shutdown and declared
force majeure in February, following a technical issue at
their plant in Marl, Germany. This further tightened European
supply.
Limited imports, tightness in feedstock nbutanol (NBA) and
the absence of BASF kept the market tight until July-August,
when seasonally weaker demand allowed supply to return to a
balanced situation.
BASF also lifted its almost year-long force majeure in
August, though production remained at reduced rates. Market
conditions returned to stability during the fourth quarter,
with balanced supply and demand largely within the
expectations of market players. It was confirmed in early
December that production of butac at Ludwigshafen had
returned to normal rates.
PRICES
In February, butac prices surged to their highest levels
since ICIS records of its price in euros began in November
1999, on news of OXEA’s declaration of force majeure and a
subsequent tightening of supply.
Feedstock NBA costs also surged to record levels in the first
half of the year on tightness largely caused by BASF
declaring force majeure on NBA from Ludwigshafen following
the explosion in October 2016. BASF is the largest producer
of NBA in Europe.
This incentivised producers to sell additional NBA rather
than using it to produce butac and supported continued high
downstream price levels. Prices steadily decreased throughout
the second half of 2017 as availability of butac and NBA
eased, but remained significantly above levels seen in 2016
before BASF declared force majeure.
TECHNOLOGY
Butac is produced by esterifying acetic acid with butanol in
the presence of sulphuric acid, which acts as a catalyst. The
acetic acid, butanol and sulphuric acid are heated in a
reactor to 89˚C (192˚F). Vapours containing butac, butanol
and water are removed and condensed.
The top layer is fed to a low boiler column where unreacted
alcohol is flashed off and recycled to the reactor. The crude
ester mixture undergoes a second distillation to separate the
butac from other byproducts.
OUTLOOK
BASF’s resumption of normal production rates at Ludwigshafen
has returned the European butac market to the structurally
long situation last seen in September 2016 where the three
major European producers (BASF, INEOS and OXEA) are all
producing at normal rates. This situation has the potential
to cause supply in Europe to become long, which would put
downwards pressure on prices.
The main question for 2018 is whether, despite this
lengthening of supply and demand likely to remain stable,
prices will remain at levels consistent with 2012-2014 or
will fall to the lower levels seen in 2015-2016. Several
sources said that they expect some downward pressure on
pricing in early 2018, though they did not believe that
prices would return to the levels seen immediately before
BASF declared force majeure in 2016.
A buyer said that it expected pressure from its downstream
customers to reduce prices now that BASF’s force majeure has
ended, which would put pressure on the prices it is paying
for butac in order to maintain its margins.
The source also said that it expected competition on pricing
from Russian and Polish producers, who were more active than
usual in northwest Europe during BASF and OXEA’s production
issues. However, upstream factors will also be a strong
influence, with higher crude oil and propylene prices
opposing the downwards pressure caused by the normalised
supply situation.
Price movements for key feedstock NBA could also be
influential on butac prices. NBA is expected to be stable to
soft but supply limitations caused by scheduled shutdowns may
limit further price decreases which could be passed through
to butac.